Abstract. Low dimensional metal oxide Nps have garnered significant attention due to their distinctive characteristics and diverse application domains. This investigation can provide further elucidation regarding the synthesis of Strontium doped-Bi2O3 efficacious photocatalysts operating under visible light, thereby potentially addressing environmental quandaries. The photoactivity of Strontium doped-Bi2O3 Nps exhibits a significantly greater magnitude when compared to that of Bi2O3 nanoparticles lacking Strontium doping. The hydrothermal method shall be employed for the synthesis of Strontium-doped Bismuth oxide in the course of preparation. A solution of NH4OH will be introduced to Bismuth nitrate and Strontium chloride. The resulting mixtures shall be subjected to vigorous stirring for a duration of 1 hour, after which they will be transferred into 100 mL autoclaves made of stainless steel and equipped with Teflon liners. These autoclaves shall then be heated to a temperature of 180 °C for a period of 6 h. The prepared samples shall subsequently undergo collection and undergo multiple washes utilising de-ionized water. In order to synthesise Strontium doped-Bi2O3 is imperative to subject the resulting compound to a subsequent calcination process at a temperature of 450° C. Infra-Red spectroscopy (FT-IR), UV-Visible, scanning electron microscopy (SEM), X-ray diffraction (XRD), techniques shall be employed for the investigation of the crystalline structures and morphologies of the powder. The resultant specimen shall subsequently serve as a catalyst for the photolytic degradation of organic dye methyl orange under diverse illumination circumstances. UV-Visible spectroscopy shall subsequently be employed to monitor the extent of photocatalytic efficacy.